| Expt No. | Volume of DMSO | Moles of Sesamol | HPLC Results | Comments |
|---|---|---|---|---|
| Expt No.15 | 6 volumes | 1.0 | 99.29% NMP 0.018% mesylate 0.22% UK RRT 1.32 |
Yield: 94.7% |
| Expt No.16 | 6 volumes | 1.5 | 99.38%NMP, 0.018 %Sesamol, 0.23 UK RRT 1 .32 |
Yield: 94.9% |
| Expt No.17 | 6 volumes | 1.1 | 99.47% NMP 0.18% UK RRT 1.04 0.26% UK RRT 1.27 |
Yield: 95.26% |
| Expt No.18 | 6 volumes | 1.3 | 99.21% NMP 0.12% UK RRT 0.63 0.3% UK RRT 1.27 |
Yield: 93.33% |